[1]王筠,刘芳,李全良,等.N-十二烷基丙烯酰胺的合成研究[J].江西师范大学学报(自然科学版),2013,(04):342-344.
　WANG Jun,LIU Fang,LI Quan-liang,et al.The Researches on Synthesis of N-Dodecylacrylamide[J].Journal of Jiangxi Normal University:Natural Science Edition,2013,(04):342-344.
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N-十二烷基丙烯酰胺的合成研究()
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《江西师范大学学报》（自然科学版）[ISSN:1006-6977/CN:61-1281/TN]

卷:
期数:
2013年04期
页码:
342-344
栏目:
出版日期:
2013-09-01

文章信息/Info

Title:
The Researches on Synthesis of N-Dodecylacrylamide
作者:
王筠;刘芳;李全良;许文俭;李铁生
周口师范学院化学系,河南周口,466000；郑州大学化学系,河南郑州,450052
Author(s):
WANG Jun；LIU Fang；LI Quan-liang；XU Wen-jian；LI Tie-sheng
关键词:
N-十二烷基丙烯酰胺; 合成; 正交试验
Keywords:
N-dodecylacrylamide; synthesis; orthogonal test
分类号:
O623
文献标志码:
A
摘要:
以十二伯胺和丙烯酸为原料在室温条件下合成N-十二烷基丙烯酰胺,其结构经IR、1H NMR鉴定表征.通过单因素实验研究了溶剂种类、反应温度、反应时间及物料配比对产物产率的影响,从而建立正交实验得出合成N-十六烷基丙烯酰胺的最优工艺条件:以氯仿为溶剂,反应温度25℃,反应时间4h,物料配比为1∶1.1时,平均产率达到80；.
Abstract:
N-dodecylacrylamide was synthesised under moderate reaction condition by dodecanamine and acrylic,which was characterized by IR and H NMR.A variety of reaction effects were investigated such as solvent type,temperature,time and feed ratio which impact on the yield.Thus the optimum reaction condition of preparation of N-dodecylacrylamide obtained by orthogonal test were as follows:using trichloromethane as solvent,reaction temperature 25 ℃,reaction time 4 h,feed ratio 1.1,the average yield reached 80%.

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备注/Memo

备注/Memo:
国家自然科学基金(20973157)
更新日期/Last Update: 1900-01-01